1. ½ÇÇèÁ¦¸ñ
°í¾Ð Batch ¹ÝÀÀ½ÇÇè°ú G.CÀÇ ¿ø¸® ¹× ½ÇÁ¦ (DMC ¿Í PhOH¸¦ ÀÌ¿ëÇÑ MPC ÇÕ¼º)
2. ½ÇÇè ¸ñÀû
°í¾Ð Batch Reactor¸¦ ÀÌ¿ëÇÑ MPCÇÕ¼ºÀÇ ¿ø¸®¸¦ ÀÌÇØÇÏ°í G.C¸¦ ÅëÇÑ ºÐ¼®À» ÅëÇØ °¢ ¼ººÐÀÇ ¸ô³óµµ¸¦ ±¸ÇÑ´Ù.
3. ½ÇÇè ÀýÂ÷
1. ½Ã·áÁغñ (mol fr. PhOH : DMC = 1:5, Ã˸Š: 10wt% TiO/SiO 0.1g)
2. Reactor Setting (300psig, 15¡É, 300RPM 500psig, 180¡É/ 40min)
3. Cooling(15¡É, 300psig/ÀÚ¿¬³Ã°¢, °Á¦³Ã°¢)
4. ½Ã·áäÃë(membrane ÀÌ¿ë)
5. °¡½º Å©·Î¸¶Åä ±×·¡ÇÇ ºÐ¼®
MPC ÇÕ¼º¿ø¸®
¡Ý ÁÖ¹ÝÀÀ
PhOH DMC MPC MeOH
PhOH MPC DPC MeOH
DMC : dimethyl carbonate
MPC : methyl phenyl carbonate
¡Ý ºÎ¹ÝÀÀ
anisole
3. ½ÇÇè Data ºÐ¼®
4.743 anisole
8.433 MPC
15.227 DPC
Reference ºÐ¼®
Weight : 18.6679g Density : 1.0306g/ml
2§¡, 2.6xxx0g
Aniso¡¦(»ý·«)
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