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Title : Synthesis of Polycarbonate.
- BPA, DPC瑜� 諛섏쓳�떆耳쒖꽌 Polycarbonate瑜� �빀�꽦�븳�떎.
1. Scheme.
1). BPA
formula : (CH3)2C(C6H4OH)2
M.W : 228.29
scheme :
2). DPC
formula : (C6H5O)2CO
M.W : 214.22
scheme :
3). reaction.
A : BPA.
B : DPC.
C : polycarbonate.
P : phenol.
2. Reagent.
- plask�뿉 BPA, DPC, catalyts瑜� �꽔�뒗�떎.
1). BPA, DPC �꽔�뒗 �뼇.
紐곗닔鍮� - BPA : DPC = 1 : 1.1
�씠踰� �떎�뿕�뿉�꽌�뒗 BPA�쓽 紐곗닔瑜� 0.05 mol濡� �븳�떎.
BPA : 0.05 mol (0.05mol 횞 228.29g/gmol = 11.4145g)
DPC : 0.055 mol (0.055mol 횞 214.22g/gmol = 11.78g)
2). Catalysts �꽔�뒗 �뼇.
紐곗닔鍮� - �쓣 留뚯”�븳�떎.
�뵲�씪�꽌 catalyst�뒗,
[catalyst] = 0.05 횞 2.5 횞 10-4 = 1.25 횞 10-5 mol. 留뚰겮�씠 �븘�슂�븯�떎.
�떎�뿕�뿉 �궗�슜�릺�뒗 catalysts.
: NaOH, Tetramethylammonium hydroxide (TMAH),
Tetraethylammonium hydroxide (TEAH), Tetrapropylammonium hydroxide (TPAH),
Tetrabutylammonium hydroxide (TBAH), Tetrabutylphophonium hydroxide (TBPH)
Example.
��� catalyst濡� NaOH瑜� �궗�슜�븷 寃쎌슦.
- NaOH ���(�깮�왂)
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